Applications of Solid-Phase Microextraction and Related Techniques

Most analytical instruments currently in use struggle to directly manage complex matrices such as environmental, food, and biological samples, making sample pretreatment essential. In the analytical process from sampling to data analysis, sample pretreatment plays a vital role in extracting, separat...

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collection Directory of Open Access Books
description Most analytical instruments currently in use struggle to directly manage complex matrices such as environmental, food, and biological samples, making sample pretreatment essential. In the analytical process from sampling to data analysis, sample pretreatment plays a vital role in extracting, separating, and concentrating target analytes. It also enhances detection, improves sensitivity and accuracy, and reduces instrument maintenance and operating costs, all of which significantly impact the reliability and accuracy of analytical results. Therefore, developing efficient sample pretreatment technologies and integrating them into various analytical instruments remains a key challenge.This reprint comprises three peer-reviewed review articles and nine original research papers contributed by research groups for a Special Issue of the MDPI journal Molecules. The topics covered include comprehensive review articles on advanced coating materials, such as metal–organic frameworks, covalent organic frameworks, hybrid graphene-based materials, and molecularly imprinted polymers. Additionally, the reprint presents various SPME and related microextraction methods employing multi-walled carbon nanotube-ionic liquid/polyaniline adsorbents, MonoTrap, covalent organic polymer mixed-matrix membranes, magnetic persimmon leaf composites, and capillary coatings as extraction materials.
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publisher MDPI - Multidisciplinary Digital Publishing Institute
publisherStr MDPI - Multidisciplinary Digital Publishing Institute
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spelling doab-20.500.12854ir-1652332025-08-12T08:15:02Z Applications of Solid-Phase Microextraction and Related Techniques Kataoka, Hiroyuki Trichosanthes anguina HS-SPME-GC-MS monoecious and diclinous plant bud volatile compound OPLS-DA polyaniline in-needle microextraction multi-walled carbon nanotube ionic liquid electrochemical polymerization solid-phase microextraction environmental analysis food analysis formaldehyde on-sample derivatization SPME SPME Arrow headspace covalent organic polymer mixed matrix membranes TpDMB-COPs membrane solid-phase extraction HPLC sulfonamides biomass adsorbent Fe3O4/persimmon leaf magnetic composite magnetic solid-phase extraction pesticides water antineoplastic drugs biological monitoring ultrahigh-performance liquid chromatography tandem mass spectrometry µSPEed micro solid phase extraction amino acids defined medium (DM) lactic acid bacteria (LAB) volatile organic compounds (VOCs) metal organic frameworks covalent organic frameworks supramolecular receptors cyclodestrins environmental monitoring graphene-based materials miniaturized sample preparation stir bar sorptive extraction microextraction by packed sorbent pipette-tip solid-phase extraction disposable pipette extraction green analytical chemistry passive smoking biomarkers cortisol in-tube solid-phase microextraction (IT-SPME) liquid chromatography–tandem mass spectrometry (LC–MS/MS) molecularly imprinted polymer (MIP) sample preparation hot mix asphalt monolithic material sorptive extraction under vacuum extraction volatile organic compounds odor emission gas chromatography-mass spectrometry n/a thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general Most analytical instruments currently in use struggle to directly manage complex matrices such as environmental, food, and biological samples, making sample pretreatment essential. In the analytical process from sampling to data analysis, sample pretreatment plays a vital role in extracting, separating, and concentrating target analytes. It also enhances detection, improves sensitivity and accuracy, and reduces instrument maintenance and operating costs, all of which significantly impact the reliability and accuracy of analytical results. Therefore, developing efficient sample pretreatment technologies and integrating them into various analytical instruments remains a key challenge.This reprint comprises three peer-reviewed review articles and nine original research papers contributed by research groups for a Special Issue of the MDPI journal Molecules. The topics covered include comprehensive review articles on advanced coating materials, such as metal–organic frameworks, covalent organic frameworks, hybrid graphene-based materials, and molecularly imprinted polymers. Additionally, the reprint presents various SPME and related microextraction methods employing multi-walled carbon nanotube-ionic liquid/polyaniline adsorbents, MonoTrap, covalent organic polymer mixed-matrix membranes, magnetic persimmon leaf composites, and capillary coatings as extraction materials. 2025-08-12T08:15:00Z 2025-08-12T08:15:00Z 2025 book ONIX_20250812T095121_9783725833788_182 9783725833788 9783725833771 https://directory.doabooks.org/handle/20.500.12854/165233 eng image/jpeg Attribution 4.0 International https://mdpi.com/books https://mdpi.com/books/pdfview/book/10629 MDPI - Multidisciplinary Digital Publishing Institute 10.3390/books978-3-7258-3377-1 10.3390/books978-3-7258-3377-1 46cabcaa-dd94-4bfe-87b4-55023c1b36d0 9783725833788 9783725833771 256 open access
spellingShingle Trichosanthes anguina
HS-SPME-GC-MS
monoecious and diclinous plant
bud
volatile compound
OPLS-DA
polyaniline
in-needle microextraction
multi-walled carbon nanotube
ionic liquid
electrochemical polymerization
solid-phase microextraction
environmental analysis
food analysis
formaldehyde
on-sample derivatization
SPME
SPME Arrow
headspace
covalent organic polymer
mixed matrix membranes
TpDMB-COPs
membrane solid-phase extraction
HPLC
sulfonamides
biomass adsorbent
Fe3O4/persimmon leaf magnetic composite
magnetic solid-phase extraction
pesticides
water
antineoplastic drugs
biological monitoring
ultrahigh-performance liquid chromatography
tandem mass spectrometry
µSPEed
micro solid phase extraction
amino acids
defined medium (DM)
lactic acid bacteria (LAB)
volatile organic compounds (VOCs)
metal organic frameworks
covalent organic frameworks
supramolecular receptors
cyclodestrins
environmental monitoring
graphene-based materials
miniaturized sample preparation
stir bar sorptive extraction
microextraction by packed sorbent
pipette-tip solid-phase extraction
disposable pipette extraction
green analytical chemistry
passive smoking
biomarkers
cortisol
in-tube solid-phase microextraction (IT-SPME)
liquid chromatography–tandem mass spectrometry (LC–MS/MS)
molecularly imprinted polymer (MIP)
sample preparation
hot mix asphalt
monolithic material sorptive extraction
under vacuum extraction
volatile organic compounds
odor emission
gas chromatography-mass spectrometry
n/a
thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general
Applications of Solid-Phase Microextraction and Related Techniques
title Applications of Solid-Phase Microextraction and Related Techniques
title_full Applications of Solid-Phase Microextraction and Related Techniques
title_fullStr Applications of Solid-Phase Microextraction and Related Techniques
title_full_unstemmed Applications of Solid-Phase Microextraction and Related Techniques
title_short Applications of Solid-Phase Microextraction and Related Techniques
title_sort applications of solid phase microextraction and related techniques
topic Trichosanthes anguina
HS-SPME-GC-MS
monoecious and diclinous plant
bud
volatile compound
OPLS-DA
polyaniline
in-needle microextraction
multi-walled carbon nanotube
ionic liquid
electrochemical polymerization
solid-phase microextraction
environmental analysis
food analysis
formaldehyde
on-sample derivatization
SPME
SPME Arrow
headspace
covalent organic polymer
mixed matrix membranes
TpDMB-COPs
membrane solid-phase extraction
HPLC
sulfonamides
biomass adsorbent
Fe3O4/persimmon leaf magnetic composite
magnetic solid-phase extraction
pesticides
water
antineoplastic drugs
biological monitoring
ultrahigh-performance liquid chromatography
tandem mass spectrometry
µSPEed
micro solid phase extraction
amino acids
defined medium (DM)
lactic acid bacteria (LAB)
volatile organic compounds (VOCs)
metal organic frameworks
covalent organic frameworks
supramolecular receptors
cyclodestrins
environmental monitoring
graphene-based materials
miniaturized sample preparation
stir bar sorptive extraction
microextraction by packed sorbent
pipette-tip solid-phase extraction
disposable pipette extraction
green analytical chemistry
passive smoking
biomarkers
cortisol
in-tube solid-phase microextraction (IT-SPME)
liquid chromatography–tandem mass spectrometry (LC–MS/MS)
molecularly imprinted polymer (MIP)
sample preparation
hot mix asphalt
monolithic material sorptive extraction
under vacuum extraction
volatile organic compounds
odor emission
gas chromatography-mass spectrometry
n/a
thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general
topic_facet Trichosanthes anguina
HS-SPME-GC-MS
monoecious and diclinous plant
bud
volatile compound
OPLS-DA
polyaniline
in-needle microextraction
multi-walled carbon nanotube
ionic liquid
electrochemical polymerization
solid-phase microextraction
environmental analysis
food analysis
formaldehyde
on-sample derivatization
SPME
SPME Arrow
headspace
covalent organic polymer
mixed matrix membranes
TpDMB-COPs
membrane solid-phase extraction
HPLC
sulfonamides
biomass adsorbent
Fe3O4/persimmon leaf magnetic composite
magnetic solid-phase extraction
pesticides
water
antineoplastic drugs
biological monitoring
ultrahigh-performance liquid chromatography
tandem mass spectrometry
µSPEed
micro solid phase extraction
amino acids
defined medium (DM)
lactic acid bacteria (LAB)
volatile organic compounds (VOCs)
metal organic frameworks
covalent organic frameworks
supramolecular receptors
cyclodestrins
environmental monitoring
graphene-based materials
miniaturized sample preparation
stir bar sorptive extraction
microextraction by packed sorbent
pipette-tip solid-phase extraction
disposable pipette extraction
green analytical chemistry
passive smoking
biomarkers
cortisol
in-tube solid-phase microextraction (IT-SPME)
liquid chromatography–tandem mass spectrometry (LC–MS/MS)
molecularly imprinted polymer (MIP)
sample preparation
hot mix asphalt
monolithic material sorptive extraction
under vacuum extraction
volatile organic compounds
odor emission
gas chromatography-mass spectrometry
n/a
thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general
url ONIX_20250812T095121_9783725833788_182