Sample Preparation-Quo Vadis

Sample preparation is and will always be the most important step in chemical analysis. Numerous techniques, methods, methodologies, and approaches are published in the literature offering a wide range of analytical tools to the lab practitioner. Analytical scientists all over the world are trying to...

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Опубликовано: MDPI - Multidisciplinary Digital Publishing Institute 2022
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Online-ссылка:ONIX_20221206_9783036557229_21
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collection Directory of Open Access Books
description Sample preparation is and will always be the most important step in chemical analysis. Numerous techniques, methods, methodologies, and approaches are published in the literature offering a wide range of analytical tools to the lab practitioner. Analytical scientists all over the world are trying to develop protocols for a plethora of analytes in various sample matrices. In the last decade, sample pre-treatment advances have followed green chemistry and green analytical chemistry demands, focusing on miniaturization and automation, using the least possible amount of organic solvents. The question is how far we have been till now, and what the future perspectives are. To answer this question, analytical chemists were invited to share their experience in the field and report on the recent advances in sample-preparation approaches. The outcome of our invitation was eleven excellent manuscripts, including four review articles and seven original research articles in the first edition of the Special Issue “Sample Preparation-Quo Vadis: Current Status of Sample Preparation Approaches”.The second edition is a collection of ten significant contributions to the field of sample preparation. It includes two highly interesting and comprehensive review articles and eight innovative research articles.
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language eng
publishDate 2022
publishDateRange 2022
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publisher MDPI - Multidisciplinary Digital Publishing Institute
publisherStr MDPI - Multidisciplinary Digital Publishing Institute
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spelling doab-20.500.12854ir-944982024-03-28T03:33:03Z Sample Preparation-Quo Vadis Samanidou, Victoria Panderi, Irene sample preparation matrix solid-phase dispersion salting-out homogenous liquid-liquid extraction bisphenol bee pollen tricyclic antidepressants urine samples bar adsorptive microextraction (BAμE) novel sorbent phases biomaterials waste flotation sampling technology GC-MS amino acids chocolate derivatization HPLC fluorescence automation flow injection inductively coupled plasma sol-gel solid-phase extraction metals molecular imprinted polymer interaction mechanism template-monomer interaction MIP-template interaction microwave-assisted extraction tocopherols phenolics flavonoids authenticity HPLC-UV bismuth oxide API particle size API morphology film-coated tablets Raman spectroscopy ImageJ tablet disintegration green extraction techniques microextraction techniques biological samples food samples environmental samples carbaryl cassia bark (Senna siamea Lam.) smartphone-based digital image analysis 1-naphthol peroxidase enzyme raman spectroscopy carriers sample holders gold layer cuvette ethanol urine volatile compounds biological fluids n/a thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general thema EDItEUR::P Mathematics and Science::PN Chemistry thema EDItEUR::P Mathematics and Science::PN Chemistry::PNF Analytical chemistry Sample preparation is and will always be the most important step in chemical analysis. Numerous techniques, methods, methodologies, and approaches are published in the literature offering a wide range of analytical tools to the lab practitioner. Analytical scientists all over the world are trying to develop protocols for a plethora of analytes in various sample matrices. In the last decade, sample pre-treatment advances have followed green chemistry and green analytical chemistry demands, focusing on miniaturization and automation, using the least possible amount of organic solvents. The question is how far we have been till now, and what the future perspectives are. To answer this question, analytical chemists were invited to share their experience in the field and report on the recent advances in sample-preparation approaches. The outcome of our invitation was eleven excellent manuscripts, including four review articles and seven original research articles in the first edition of the Special Issue “Sample Preparation-Quo Vadis: Current Status of Sample Preparation Approaches”.The second edition is a collection of ten significant contributions to the field of sample preparation. It includes two highly interesting and comprehensive review articles and eight innovative research articles. 2022-12-06T16:08:26Z 2022-12-06T16:08:26Z 2022 book ONIX_20221206_9783036557229_21 9783036557229 9783036557212 https://directory.doabooks.org/handle/20.500.12854/94498 eng image/jpeg Attribution 4.0 International https://mdpi.com/books/pdfview/book/6322 https://mdpi.com/books/pdfview/book/6322 MDPI - Multidisciplinary Digital Publishing Institute 10.3390/books978-3-0365-5721-2 10.3390/books978-3-0365-5721-2 46cabcaa-dd94-4bfe-87b4-55023c1b36d0 9783036557229 9783036557212 186 Basel open access
spellingShingle sample preparation
matrix solid-phase dispersion
salting-out
homogenous liquid-liquid extraction
bisphenol
bee pollen
tricyclic antidepressants
urine samples
bar adsorptive microextraction (BAμE)
novel sorbent phases
biomaterials waste
flotation sampling technology
GC-MS
amino acids
chocolate
derivatization
HPLC
fluorescence
automation
flow injection
inductively coupled plasma
sol-gel
solid-phase extraction
metals
molecular imprinted polymer
interaction mechanism
template-monomer interaction
MIP-template interaction
microwave-assisted extraction
tocopherols
phenolics
flavonoids
authenticity
HPLC-UV
bismuth oxide
API particle size
API morphology
film-coated tablets
Raman spectroscopy
ImageJ
tablet disintegration
green extraction techniques
microextraction techniques
biological samples
food samples
environmental samples
carbaryl
cassia bark (Senna siamea Lam.)
smartphone-based digital image analysis
1-naphthol
peroxidase enzyme
raman spectroscopy
carriers
sample holders
gold layer
cuvette
ethanol
urine
volatile compounds
biological fluids
n/a
thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general
thema EDItEUR::P Mathematics and Science::PN Chemistry
thema EDItEUR::P Mathematics and Science::PN Chemistry::PNF Analytical chemistry
Sample Preparation-Quo Vadis
title Sample Preparation-Quo Vadis
title_full Sample Preparation-Quo Vadis
title_fullStr Sample Preparation-Quo Vadis
title_full_unstemmed Sample Preparation-Quo Vadis
title_short Sample Preparation-Quo Vadis
title_sort sample preparation quo vadis
topic sample preparation
matrix solid-phase dispersion
salting-out
homogenous liquid-liquid extraction
bisphenol
bee pollen
tricyclic antidepressants
urine samples
bar adsorptive microextraction (BAμE)
novel sorbent phases
biomaterials waste
flotation sampling technology
GC-MS
amino acids
chocolate
derivatization
HPLC
fluorescence
automation
flow injection
inductively coupled plasma
sol-gel
solid-phase extraction
metals
molecular imprinted polymer
interaction mechanism
template-monomer interaction
MIP-template interaction
microwave-assisted extraction
tocopherols
phenolics
flavonoids
authenticity
HPLC-UV
bismuth oxide
API particle size
API morphology
film-coated tablets
Raman spectroscopy
ImageJ
tablet disintegration
green extraction techniques
microextraction techniques
biological samples
food samples
environmental samples
carbaryl
cassia bark (Senna siamea Lam.)
smartphone-based digital image analysis
1-naphthol
peroxidase enzyme
raman spectroscopy
carriers
sample holders
gold layer
cuvette
ethanol
urine
volatile compounds
biological fluids
n/a
thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general
thema EDItEUR::P Mathematics and Science::PN Chemistry
thema EDItEUR::P Mathematics and Science::PN Chemistry::PNF Analytical chemistry
topic_facet sample preparation
matrix solid-phase dispersion
salting-out
homogenous liquid-liquid extraction
bisphenol
bee pollen
tricyclic antidepressants
urine samples
bar adsorptive microextraction (BAμE)
novel sorbent phases
biomaterials waste
flotation sampling technology
GC-MS
amino acids
chocolate
derivatization
HPLC
fluorescence
automation
flow injection
inductively coupled plasma
sol-gel
solid-phase extraction
metals
molecular imprinted polymer
interaction mechanism
template-monomer interaction
MIP-template interaction
microwave-assisted extraction
tocopherols
phenolics
flavonoids
authenticity
HPLC-UV
bismuth oxide
API particle size
API morphology
film-coated tablets
Raman spectroscopy
ImageJ
tablet disintegration
green extraction techniques
microextraction techniques
biological samples
food samples
environmental samples
carbaryl
cassia bark (Senna siamea Lam.)
smartphone-based digital image analysis
1-naphthol
peroxidase enzyme
raman spectroscopy
carriers
sample holders
gold layer
cuvette
ethanol
urine
volatile compounds
biological fluids
n/a
thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general
thema EDItEUR::P Mathematics and Science::PN Chemistry
thema EDItEUR::P Mathematics and Science::PN Chemistry::PNF Analytical chemistry
url ONIX_20221206_9783036557229_21