Solid-Phase Microextraction and Related Techniques in Bioanalysis
Bioanalysis of endogenous substances, metabolites, and contaminants poisons is important in analyses of biological functions, metabolomics, forensic toxicology, patient diagnosis and biomonitoring of human exposure to hazardous chemicals. In these analyses, methods of sample preparation are essentia...
সংরক্ষণ করুন:
| বিন্যাস: | Online |
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| ভাষা: | ইংরেজি |
| প্রকাশিত: |
MDPI - Multidisciplinary Digital Publishing Institute
2023
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| বিষয়গুলি: | |
| অনলাইন ব্যবহার করুন: | ONIX_20230405_9783036570471_204 |
| ট্যাগগুলো: |
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| _version_ | 1869520089869451264 |
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| collection | Directory of Open Access Books |
| description | Bioanalysis of endogenous substances, metabolites, and contaminants poisons is important in analyses of biological functions, metabolomics, forensic toxicology, patient diagnosis and biomonitoring of human exposure to hazardous chemicals. In these analyses, methods of sample preparation are essential for the isolation and concentration of target analytes from complex biological matrices. These processes, however, are time-consuming, labor-intensive and error-prone, and markedly influence the reliability and accuracy of determining target analytes. Thus, efficient sample preparation techniques and their integration with analytical methods have become significant. Solid-phase microextraction (SPME) is a simple and convenient sample preparation technique that has enabled automation, miniaturization, high-throughput performance, and online coupling with analytical instruments. Moreover, SPME has reduced analysis times, as well as solvent and disposal costs.This reprint consists of 14 original, peer-reviewed papers for the Special Issue in the MDPI journal Molecules. The topics covered include headspace fiber SPME (HS-SPME) gas chromatography-mass spectrometry (GC-MS), HS-in-needle microextraction GC-MS, thin film SPME liquid chromatography-tandem mass spectrometry (LC-MS/MS), magnetic solid phase extraction LC-MS/MS, in-tube SPME LC-MS/MS and in-tube SPME LC-UV. Samples analyzed include plant-derived volatile organic compounds; body odor; metabolites in urine, plasma and saliva sample; and biomarkers of tobacco smoke exposure in hair and environmental estrogens. |
| format | Online |
| id | doab-20.500.12854ir-98925 |
| institution | Directory of Open Access Books |
| language | eng |
| publishDate | 2023 |
| publishDateRange | 2023 |
| publishDateSort | 2023 |
| publisher | MDPI - Multidisciplinary Digital Publishing Institute |
| publisherStr | MDPI - Multidisciplinary Digital Publishing Institute |
| record_format | ojs |
| spelling | doab-20.500.12854ir-989252024-03-28T03:33:01Z Solid-Phase Microextraction and Related Techniques in Bioanalysis Kataoka, Hiroyuki tobacco-specific nitrosamines hair exposure biomarkers in-tube solid-phase microextraction (SPME) liquid chromatography-tandem mass spectrometry (LC–MS/MS) bioanalysis carbon materials HPLC–MS biological matrices solid-phase extraction sample preparation bladder cancer (BC) metabolomics solid phase microextraction (SPME) liquid chromatography mass spectrometry urine Myrtaceae native fruit volatile compounds sesquiterpenes body odor 2-nonenal wiping method pasting method solid-phase microextraction (HS–SPME) gas chromatography–mass spectrometry (GC–MS) passive smoking nicotine cotinine risk assessment headspace solid-phase microextraction Cerrado aroma volatile organic compounds Herpetospermum pedunculosum HS-SPME-GC-MS dioecious plant bud volatile compound multivariate statistical analysis green peach aphids VOCs parasitoids Aphidus colemani Aphelinus abdominalis cabbage cerrado Anacardiaceae aroeira biological properties virtual screening chemoinformatics volatile organic compounds (VOCs) headspace solid-phase microextraction (HS-SPME) SPME-GC-MS stored-product insect pests Tribolium castaneum Rhyzopertha dominica Sitophilus granarius titanium wire superhydrophobic superhydrophilic in-tube solid-phase microextraction high-performance liquid chromatography sulfated steroid metabolites saliva online automated analysis in-tube solid-phase microextraction (IT-SPME) liquid chromatography–tandem mass spectrometry (LC–MS/MS) stable isotope dilution human body odor GO:PANI/ZNRs/ZIF−8 response surface methodology needle-based adsorbent headspace-in needle microextraction n/a thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general thema EDItEUR::P Mathematics and Science::PN Chemistry thema EDItEUR::P Mathematics and Science::PN Chemistry::PNF Analytical chemistry Bioanalysis of endogenous substances, metabolites, and contaminants poisons is important in analyses of biological functions, metabolomics, forensic toxicology, patient diagnosis and biomonitoring of human exposure to hazardous chemicals. In these analyses, methods of sample preparation are essential for the isolation and concentration of target analytes from complex biological matrices. These processes, however, are time-consuming, labor-intensive and error-prone, and markedly influence the reliability and accuracy of determining target analytes. Thus, efficient sample preparation techniques and their integration with analytical methods have become significant. Solid-phase microextraction (SPME) is a simple and convenient sample preparation technique that has enabled automation, miniaturization, high-throughput performance, and online coupling with analytical instruments. Moreover, SPME has reduced analysis times, as well as solvent and disposal costs.This reprint consists of 14 original, peer-reviewed papers for the Special Issue in the MDPI journal Molecules. The topics covered include headspace fiber SPME (HS-SPME) gas chromatography-mass spectrometry (GC-MS), HS-in-needle microextraction GC-MS, thin film SPME liquid chromatography-tandem mass spectrometry (LC-MS/MS), magnetic solid phase extraction LC-MS/MS, in-tube SPME LC-MS/MS and in-tube SPME LC-UV. Samples analyzed include plant-derived volatile organic compounds; body odor; metabolites in urine, plasma and saliva sample; and biomarkers of tobacco smoke exposure in hair and environmental estrogens. 2023-04-05T12:59:21Z 2023-04-05T12:59:21Z 2023 book ONIX_20230405_9783036570471_204 9783036570471 9783036570464 https://directory.doabooks.org/handle/20.500.12854/98925 eng application/octet-stream Attribution 4.0 International https://mdpi.com/books/pdfview/book/6978 https://mdpi.com/books/pdfview/book/6978 MDPI - Multidisciplinary Digital Publishing Institute 10.3390/books978-3-0365-7046-4 10.3390/books978-3-0365-7046-4 46cabcaa-dd94-4bfe-87b4-55023c1b36d0 9783036570471 9783036570464 198 Basel open access |
| spellingShingle | tobacco-specific nitrosamines hair exposure biomarkers in-tube solid-phase microextraction (SPME) liquid chromatography-tandem mass spectrometry (LC–MS/MS) bioanalysis carbon materials HPLC–MS biological matrices solid-phase extraction sample preparation bladder cancer (BC) metabolomics solid phase microextraction (SPME) liquid chromatography mass spectrometry urine Myrtaceae native fruit volatile compounds sesquiterpenes body odor 2-nonenal wiping method pasting method solid-phase microextraction (HS–SPME) gas chromatography–mass spectrometry (GC–MS) passive smoking nicotine cotinine risk assessment headspace solid-phase microextraction Cerrado aroma volatile organic compounds Herpetospermum pedunculosum HS-SPME-GC-MS dioecious plant bud volatile compound multivariate statistical analysis green peach aphids VOCs parasitoids Aphidus colemani Aphelinus abdominalis cabbage cerrado Anacardiaceae aroeira biological properties virtual screening chemoinformatics volatile organic compounds (VOCs) headspace solid-phase microextraction (HS-SPME) SPME-GC-MS stored-product insect pests Tribolium castaneum Rhyzopertha dominica Sitophilus granarius titanium wire superhydrophobic superhydrophilic in-tube solid-phase microextraction high-performance liquid chromatography sulfated steroid metabolites saliva online automated analysis in-tube solid-phase microextraction (IT-SPME) liquid chromatography–tandem mass spectrometry (LC–MS/MS) stable isotope dilution human body odor GO:PANI/ZNRs/ZIF−8 response surface methodology needle-based adsorbent headspace-in needle microextraction n/a thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general thema EDItEUR::P Mathematics and Science::PN Chemistry thema EDItEUR::P Mathematics and Science::PN Chemistry::PNF Analytical chemistry Solid-Phase Microextraction and Related Techniques in Bioanalysis |
| title | Solid-Phase Microextraction and Related Techniques in Bioanalysis |
| title_full | Solid-Phase Microextraction and Related Techniques in Bioanalysis |
| title_fullStr | Solid-Phase Microextraction and Related Techniques in Bioanalysis |
| title_full_unstemmed | Solid-Phase Microextraction and Related Techniques in Bioanalysis |
| title_short | Solid-Phase Microextraction and Related Techniques in Bioanalysis |
| title_sort | solid phase microextraction and related techniques in bioanalysis |
| topic | tobacco-specific nitrosamines hair exposure biomarkers in-tube solid-phase microextraction (SPME) liquid chromatography-tandem mass spectrometry (LC–MS/MS) bioanalysis carbon materials HPLC–MS biological matrices solid-phase extraction sample preparation bladder cancer (BC) metabolomics solid phase microextraction (SPME) liquid chromatography mass spectrometry urine Myrtaceae native fruit volatile compounds sesquiterpenes body odor 2-nonenal wiping method pasting method solid-phase microextraction (HS–SPME) gas chromatography–mass spectrometry (GC–MS) passive smoking nicotine cotinine risk assessment headspace solid-phase microextraction Cerrado aroma volatile organic compounds Herpetospermum pedunculosum HS-SPME-GC-MS dioecious plant bud volatile compound multivariate statistical analysis green peach aphids VOCs parasitoids Aphidus colemani Aphelinus abdominalis cabbage cerrado Anacardiaceae aroeira biological properties virtual screening chemoinformatics volatile organic compounds (VOCs) headspace solid-phase microextraction (HS-SPME) SPME-GC-MS stored-product insect pests Tribolium castaneum Rhyzopertha dominica Sitophilus granarius titanium wire superhydrophobic superhydrophilic in-tube solid-phase microextraction high-performance liquid chromatography sulfated steroid metabolites saliva online automated analysis in-tube solid-phase microextraction (IT-SPME) liquid chromatography–tandem mass spectrometry (LC–MS/MS) stable isotope dilution human body odor GO:PANI/ZNRs/ZIF−8 response surface methodology needle-based adsorbent headspace-in needle microextraction n/a thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general thema EDItEUR::P Mathematics and Science::PN Chemistry thema EDItEUR::P Mathematics and Science::PN Chemistry::PNF Analytical chemistry |
| topic_facet | tobacco-specific nitrosamines hair exposure biomarkers in-tube solid-phase microextraction (SPME) liquid chromatography-tandem mass spectrometry (LC–MS/MS) bioanalysis carbon materials HPLC–MS biological matrices solid-phase extraction sample preparation bladder cancer (BC) metabolomics solid phase microextraction (SPME) liquid chromatography mass spectrometry urine Myrtaceae native fruit volatile compounds sesquiterpenes body odor 2-nonenal wiping method pasting method solid-phase microextraction (HS–SPME) gas chromatography–mass spectrometry (GC–MS) passive smoking nicotine cotinine risk assessment headspace solid-phase microextraction Cerrado aroma volatile organic compounds Herpetospermum pedunculosum HS-SPME-GC-MS dioecious plant bud volatile compound multivariate statistical analysis green peach aphids VOCs parasitoids Aphidus colemani Aphelinus abdominalis cabbage cerrado Anacardiaceae aroeira biological properties virtual screening chemoinformatics volatile organic compounds (VOCs) headspace solid-phase microextraction (HS-SPME) SPME-GC-MS stored-product insect pests Tribolium castaneum Rhyzopertha dominica Sitophilus granarius titanium wire superhydrophobic superhydrophilic in-tube solid-phase microextraction high-performance liquid chromatography sulfated steroid metabolites saliva online automated analysis in-tube solid-phase microextraction (IT-SPME) liquid chromatography–tandem mass spectrometry (LC–MS/MS) stable isotope dilution human body odor GO:PANI/ZNRs/ZIF−8 response surface methodology needle-based adsorbent headspace-in needle microextraction n/a thema EDItEUR::G Reference, Information and Interdisciplinary subjects::GP Research and information: general thema EDItEUR::P Mathematics and Science::PN Chemistry thema EDItEUR::P Mathematics and Science::PN Chemistry::PNF Analytical chemistry |
| url | ONIX_20230405_9783036570471_204 |